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Abstract:

Structural control in micro- and nanometer scales is necessary to design highly functional materials. Crystalline mesoporous microspheres (MMSs) are expected to improve electrochemical, catalytic, and adsorption performances. In this study, we focused on the preparation of templated MMSs of nickel-based layered hydroxides by using pre-crystallized nano-building blocks (NBBs). Layered nickel hydroxide nanoparticles were prepared through an epoxide-mediated alkalinization process and used as NBBs to construct microspheres. The spherical particles in micrometer scale were synthesized by an aerosol-assisted assembly of the NBBs dispersed in a solvent, in the presence of supramolecular templates. It was found that controlling the crystallization as well as the surface philicity permits to yield the NBBs with an adequately small size and interparticle interactions that generate self-assembled MMSs akin to those obtained in NBB-based mesoporous thin films. The preparation technique demonstrated here is highly versatile; templated MMSs with various chemical compositions of nickel-based layered double hydroxides were successfully obtained. [Figure not available: see fulltext.] © 2018, Springer Science+Business Media, LLC, part of Springer Nature.

Registro:

Documento: Artículo
Título:Mesoporous microspheres of nickel-based layered hydroxides by aerosol-assisted self-assembly using crystalline nano-building blocks
Autor:Tarutani, N.; Tokudome, Y.; Jobbágy, M.; Soler-Illia, G.J.A.A.; Takahashi, M.
Filiación:Department of Materials Science, Graduate School of Engineering, Osaka Prefecture University, Sakai, Osaka 599-8531, Japan
INQUIMAE-CONICET, Facultad Ciencias Exactas y Naturales, Universidad de Buenos Aires, Buenos Aires, C1428EHA, Argentina
Instituto de Nanosistemas, Universidad Nacional de General San Martín-CONICET, Av. 25 de Mayo y Francia, San Martín 1650, Buenos Aires, Argentina
Department of Chemical Science and Technology, Faculty of Bioscience and Applied Chemistry, Hosei University, Koganei, Tokyo 184-8584, Japan
Palabras clave:Crystalline mesoporous microspheres; Epoxide-mediated alkalinization; Layered double hydroxides; Layered nickel hydroxides; Nano-building blocks; Aerosols; Association reactions; Crystalline materials; Film preparation; Functional materials; Mesoporous materials; Microspheres; Self assembly; Structural dynamics; Crystalline mesoporous; Epoxide-mediated alkalinization; Layered double hydroxides; Nanobuilding blocks; Nickel hydroxides; Nickel compounds
Año:2019
Volumen:89
Número:1
Página de inicio:216
Página de fin:224
DOI: http://dx.doi.org/10.1007/s10971-018-4810-z
Título revista:Journal of Sol-Gel Science and Technology
Título revista abreviado:J Sol Gel Sci Technol
ISSN:09280707
CODEN:JSGTE
Registro:http://digital.bl.fcen.uba.ar/collection/paper/document/paper_09280707_v89_n1_p216_Tarutani

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Citas:

---------- APA ----------
Tarutani, N., Tokudome, Y., Jobbágy, M., Soler-Illia, G.J.A.A. & Takahashi, M. (2019) . Mesoporous microspheres of nickel-based layered hydroxides by aerosol-assisted self-assembly using crystalline nano-building blocks. Journal of Sol-Gel Science and Technology, 89(1), 216-224.
http://dx.doi.org/10.1007/s10971-018-4810-z
---------- CHICAGO ----------
Tarutani, N., Tokudome, Y., Jobbágy, M., Soler-Illia, G.J.A.A., Takahashi, M. "Mesoporous microspheres of nickel-based layered hydroxides by aerosol-assisted self-assembly using crystalline nano-building blocks" . Journal of Sol-Gel Science and Technology 89, no. 1 (2019) : 216-224.
http://dx.doi.org/10.1007/s10971-018-4810-z
---------- MLA ----------
Tarutani, N., Tokudome, Y., Jobbágy, M., Soler-Illia, G.J.A.A., Takahashi, M. "Mesoporous microspheres of nickel-based layered hydroxides by aerosol-assisted self-assembly using crystalline nano-building blocks" . Journal of Sol-Gel Science and Technology, vol. 89, no. 1, 2019, pp. 216-224.
http://dx.doi.org/10.1007/s10971-018-4810-z
---------- VANCOUVER ----------
Tarutani, N., Tokudome, Y., Jobbágy, M., Soler-Illia, G.J.A.A., Takahashi, M. Mesoporous microspheres of nickel-based layered hydroxides by aerosol-assisted self-assembly using crystalline nano-building blocks. J Sol Gel Sci Technol. 2019;89(1):216-224.
http://dx.doi.org/10.1007/s10971-018-4810-z